超声与振荡提取沉积物中松散结合态磷的比较     

罗俊凌罗爱芹  张月琴 《岩矿测试》2005,24(3):193-196

用超声技术提取沉积物样品中松散结合态磷,并与振荡提取结果进行比较。结果表明,超声提取结果与振荡提取结果大致相当。超声提取耗时短,操作简单易行,测试结果精密度为3.8%(RSD,n=7),可以替代振荡方法提取沉积物中的松散结合态磷。  相似文献   

声波扫描成像在灾害防治及环境保护中的应用     

韩绪山  张景考 《中国煤田地质》2003,15(2):59-62,66

利用超声波扫描成像测井技术，在地质灾害的预防与环境保护中可以检测由于采矿而形成的冒落带、裂隙带、离层带、洞穴及软弱层的存在状况及部位，测定基岩风化蚀变程度及深度，在地质灾害与环境保护的治理时可以监测治理的质量，提供了直观精确可靠的基础资料。  相似文献   

超声提取-气相色谱法测定覆盖区土壤中的六六六和滴滴涕   总被引：4，自引：2，他引：4  

李军 《岩矿测试》2003,22(4):248-253

将超声波提取技术引入到覆盖区土壤样品六六六、滴滴涕组分的预处理中，建立了超声提取，磺化法净化，气相色谱测定的分析方法。对被测组分在超声波提取中的稳定性进行了试验，对超声提取时间、提取温度、提取溶剂用量以及磺化净化过程可能导致组分损失的各种相关条件逐个试验筛选，采用样品加标回收法对六六六、滴滴涕的8种组分进行了两种浓度的精密度和准确度试验，RSD值均小于10％，平均回收率92．5％-103．9％。方法对各种异构体的六六六、滴滴涕的最低检测浓度为0．30-3．89ng／g。  相似文献   

天然含钒金红石加热、淬火及电子辐射改性实验研究   总被引：4，自引：5，他引：4       下载免费PDF全文

刘娟鲁安怀  郭延军李宁  李巧荣郑佳 《岩石矿物学杂志》2003,22(4):339-344

天然含钒金红石样品经过1273K加热、淬火和高能电子辐照处理后性质发生不同程度的变化。XRD谱峰显示处理前后样品没有发生物相变化，显微IR图谱证明原样、加热、淬火样品的表面有少量吸附水存在，而辐射样品的显微IR图谱上没有检测到吸附水的吸收峰。用XPS分析比较了处理前后样品表面主要元素Ti、O和V的价态及含量，结果表明，原样经过处理后表面钒和氧的原子百分含量增加，其中淬火样品表面吸附水和钒的含量相对于原样增加最为明显，光催化活性相应较高；加热样品表面的吸附水和钒的含量比原样稍有增加，光催化活性与原样相当；电子辐射样品表面钒的原子百分含量相对原样增加不明显，而对水的吸附能力相对原样较低，光催化效率也略低。  相似文献   

High Pressure-Differential Thermal Analysis and Ultrasonic Wave Amplitude Analysis of Ice-Water Equilibrium at 1.5-5.0GPa     

Xu Yousheng  Zheng Haifei  Xie Hongsen  Zhang Yueming  Xu Huigang  Guo Jie 《中国地球化学学报》1996,15(2):153-158

Water is the most active component in all geological systems.It has an important effect on the physical properties of minerals and melts.It also plays a key role in the evolution of the Earth.Accurate thermodynamics data on water are currently confined to pressures below 1.0GPa and temperatures below 900℃.Presented in this paper are new data available on the P-T properties of water at pressures up to 5.0GPa,develoged from differential thermal analysis and ultrasonic wave amplitude analysis.It has been found that there may exist another ternary point at 3.0GPa and that ultrasonic wave amplitude change of ice-water transition shows two inflection points above 2.0GPa, consistent with the two peaks of differential thermal curves above 2.0GPa .It may be a new phenomenon which needs further study.  相似文献   

Some effects of the memory kernel singularity on wave propagation and inversion in viscoelastic media – II. Inversion     

A. Ribodetti  A. Hanyga 《Geophysical Journal International》2004,158(2):426-442

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采空区二维超声波物理模型实验研究     

赵家福  田钢  石战结  王者江 《吉林大学学报(地球科学版)》2005,(Z1)

由于对资源矿产的过度开采使得矿山地区(尤其是煤矿)出现了采空区,从而引起地表塌陷等地质灾害。为了深入了解地震方法在采空区调查中的应用效果,从超声波物理模型实验研究出发,论述了物理模型的原理和制作,研究了采空区的地震波场特征,并利用W inse is软件对所采集的二维超声波实验数据进行了处理。由叠偏剖面推断的采空区的位置与实际模型相符,从而验证了超声波采空区物理模型试验是有效的、可信的;同时可以为实际探测采空区提供进一步的理论依据。  相似文献   

Retention of cosmogenic 3He in calcite     

《Quaternary Geochronology》2015

Cosmogenic ³He can be used to date a wide range of mineral phases because it is produced from all target elements and can be readily measured above atmospheric contamination. Calcite is a particularly attractive target mineral due to its natural abundance, large crystal size (>1 mm), and low He closure temperature (<70 °C), which limit non-cosmogenic ³He components (Copeland et al., 2007). However, several recent studies have shown that some calcite may not be retentive to helium, even under surface temperatures (Cros et al., 2014; Copeland et al., 2007). This study thus explores ³He retention and production in natural calcite samples at four different sites. Samples from two high elevation sites appear retentive to ³He over 10 kyr timescales, whereas two additional sites clearly suffer from diffusive loss of ³He. Step-degassing experiments suggest that diffusion in calcite is controlled by multiple diffusion domains, with an apparent activation energy of 25–27 kcal mol⁻¹. Although minor ³He loss is expected from the smallest diffusion domains, the observed kinetics cannot explain the poor retention at all sites. We thus propose that opaque (non-transparent) calcite may be more retentive due to the presence of imperfections in the crystal lattice. We conclude that ³He dating of calcite shows promise in some settings. However, because retention depends on crystallographic variability it must be evaluated on a case-by-case basis until robust criteria for retention can be identified.  相似文献   

Brillouin scattering study on elastic and piezoelectric properties of laser irradiated ZnO single crystals     

刘洁  蒋毅坚 《海洋学报(英文版)》2010,29(11)

Brillouin light scattering technique can be successfully used to determine the whole set of elastic and piezoelectric constants of a ZnO single crystal irradiated by different laser energy densities, into a micron range (radiation layer thickness). It is found that the scattering intensity, the linewidth and the Brillouin scattering shift of acoustic phonons are all strongly dependent on laser energy density. Based on the sound propagation equations and these results, the directional dependences of the compressional and shear moduli of the irradiated ZnO sample in the (001) plane are investigated. It is found that under an appropriate laser condition, 248 nm KrF excimer laser irradiation can significantly improve the surface quality and increase the elastic properties of ZnO single crystal. This procedure has potential applications in the fabrication of ZnO-based surface acoustic wave and optic-electronic devices.  相似文献   

超声波测风仪风速的不同算法误差分析     

涂满红  曹云昌  詹国伟  赤桑单吉 《气象与环境科学》2019,42(1):119-126

超声波测风仪与气象业务用风向标测风仪相比具有诸多优势,可为气象业务中风向风速观测急需解决的较多问题提供解决方案。为促成超声波风速仪尽早在气象部门业务应用,同时解决资料同化等问题,研究和选择适用于超声波测风仪的风速平均(平滑)算法显得极为重要。为此,从超声波测风仪测量原理出发,介绍了超声波测风仪获取数据的特点;利用台站获取的超声波测风仪风速的秒数据,采用不同时段、不同平均(平滑)方法,计算风速多种形式的平均值,通过统计、分析和比较,获得了标量和矢量不同算法下风速平均值的特性差异及其之间的误差,进一步验证了标量平均大于矢量平均的结论。通过对超声波测风仪的风速算法研究及其误差分析,对减小因算法带来的风速测量误差提供方法,同时探讨了超声波测风仪在气象业务使用的可能和方向。  相似文献